4-Nitrobenzaldehyde → HCID 59262210, compound

HRID 906375Notes

Reaction equation

HRID 906375 reaction equation
[N+:1]([C:4]1[CH:11]=[CH:10][C:7]([CH:8]=O)=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH3:12][C@@H:13]1[CH2:18][NH:17][CH2:16][C@H:15]([CH3:19])[NH:14]1>>[N+:1]([C:4]1[CH:11]=[CH:10][C:7]([CH2:8][N:17]2[CH2:16][C@H:15]([CH3:19])[NH:14][C@H:13]([CH3:12])[CH2:18]2)=[CH:6][CH:5]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 5414-NitrobenzaldehydeHCID 6950261rel-(2R,6S)-2,6-dimethylpiperazine

Product 1

HCID 59262210HCID 59262210, compound

Procedure

The title compound was prepared from 4-nitrobenzaldehyde and (2R,6S)-2,6-dimethylpiperazine using a method similar to that described for D21 in Description 21A. MS (ES): MH+ 250.2.

Sources & evidence

ORD record
ord-7416cc4c8b7d43bd90b8abc26600a64b
Source dataset
uspto-grants-2011_09
Patent number
US08012981B2

Reaction notes

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