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HRID917888

反应详情

EQUATION

反应方程式

HRID 917888 的结构方程式

REACTANTS

反应物

4
结构：Oc1ccccc1
HCID996

Phenol

C6H6O

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CC(CCO)CCO
HCID20524

3-Methyl-1,5-pentanediol

C6H14O2

结构：Nc1c(Cl)cc(O)c2c1C(=O)c1ccccc1C2=O
HCID75590

9,10-Anthracenedione, 1-amino-2-chloro-4-hydroxy-

C14H8ClNO3

PRODUCTS

生成物

1
结构：CC(CCO)CCOc1cc(O)c2c(c1N)C(=O)c1ccccc1C2=O
HCID21524107

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN1CCCC1=O
溶剂HCID13387

N-Methyl-2-pyrrolidone

C5H9NO

CONDITIONS

反应条件

温度
140 °C

PROCEDURE

实验过程

A mixture of 25 parts of 3-methyl-1,5-pentanediol, 12 parts of N-methylpyrrolidone, 2.6 parts of phenol and 3.3 parts of potassium carbonate is mixed with 8 parts of 1-amino-4-hydroxy-2-chloroanthraquinone at 130°C and stirred for 3 hours at 130°C and 2 hours at 140°C under nitrogen. After working up, 6 parts of 1-amino-2-(5'-hydroxy-3'-methylpentoxy)-4-hydroxyanthraquinone melting at from 134° to 135°C are obtained.