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HRID917890

反应详情

EQUATION

反应方程式

HRID 917890 的结构方程式

REACTANTS

反应物

4
结构：OCCO
HCID174

Ethylene glycol

C2H6O2

结构：Oc1ccccc1
HCID996

Phenol

C6H6O

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Nc1c(Cl)cc(O)c2c1C(=O)c1ccccc1C2=O
HCID75590

9,10-Anthracenedione, 1-amino-2-chloro-4-hydroxy-

C14H8ClNO3

PRODUCTS

生成物

1
结构：Nc1c(OCCO)cc(O)c2c1C(=O)c1ccccc1C2=O
HCID87341

9,10-Anthracenedione, 1-amino-4-hydroxy-2-(2-hydroxyethoxy)-

C16H13NO5

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN1CCCC1=O
溶剂HCID13387

N-Methyl-2-pyrrolidone

C5H9NO

PROCEDURE

实验过程

47 parts of ethylene glycol, 13.7 parts of 1-amino-4-hydroxy-2-chloroanthraquinone, 24 parts of N-methylpyrrolidone, 1.2 parts of phenol and 6 parts of potassium carbonate are heated for 6 hours at 120°-125°C under nitrogen. After working up, 10.5 parts of 1-amino-2-(2'-hydroxyethoxy)-4-hydroxyanthraquinone are obtained.