HRID926814

反应详情

EQUATION

反应方程式

HRID 926814 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The synthesis of MA-GG-TT was similar to the synthesis of MA-GFLG-TT in Example 1. N-methacryloylglycylglycine (MA-GG-OH) was coupled with 2-mercaptothiazoline in DCM mediated by EDCI in presence of catalytic amount of DMAP. After reaction, the product was purified by recrystallization from MeOH solution.

WORKUP

后处理

  1. customThe synthesis of MA-GG-TT
  2. customwas similar to the synthesis of MA-GFLG-TT in Example 1
  3. customAfter reaction
  4. customthe product was purified by recrystallization from MeOH solution