HRID926814
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The synthesis of MA-GG-TT was similar to the synthesis of MA-GFLG-TT in Example 1. N-methacryloylglycylglycine (MA-GG-OH) was coupled with 2-mercaptothiazoline in DCM mediated by EDCI in presence of catalytic amount of DMAP. After reaction, the product was purified by recrystallization from MeOH solution.
WORKUP
后处理
- customThe synthesis of MA-GG-TT
- customwas similar to the synthesis of MA-GFLG-TT in Example 1
- customAfter reaction
- customthe product was purified by recrystallization from MeOH solution