Sodium ion → tert-Butyl 3-(azidomethyl)piperidine-1-carboxylate

HRID 937268Notes

Reaction equation

HRID 937268 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH:10]([CH2:14][O:15][S:16]([CH3:17])(=[O:18])=[O:19])[CH2:11][CH2:12][CH2:13]1.[CH3:24][N:25]([CH3:26])[CH:27]=[O:28].[N-:21]=[N+:22]=[N-:23].[Na+:20]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH:10]([CH2:14][N:21]=[N+:22]=[N-:23])[CH2:11][CH2:12][CH2:13]1

Participants

5

Reactant 4

HCID 923Sodium ionHCID 6228DimethylformamideHCID 33558AzideHCID 22647269tert-Butyl 3-(((methylsulfonyl)oxy)methyl)piperidine-1-carboxylate

Product 1

HCID 22647380tert-Butyl 3-(azidomethyl)piperidine-1-carboxylate

Sources & evidence

ORD record
ord-241513d23b67477f9d3d41c755f520a1
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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