Acetic Acid → 2-Bromo-1-(oxan-4-yl)ethan-1-one

HRID 940895Notes

Reaction equation

HRID 940895 reaction equation
[BrH:21].[CH3:14][Si:15]([CH:16]=[N+:17]=[N-:18])([CH3:19])[CH3:20].[CH3:22][C:23](=[O:24])[OH:25].[O:5]1[CH2:6][CH2:7][CH:8]([C:11](=[O:12])[OH:13])[CH2:9][CH2:10]1.[S:1]([Cl:2])([Cl:3])=[O:4]>>[O:5]1[CH2:6][CH2:7][CH:8]([C:11](=[O:13])[CH2:14][Br:21])[CH2:9][CH2:10]1

Participants

6

Reactant 5

HCID 176Acetic AcidHCID 260Hydrogen BromideHCID 24386Thionyl ChlorideHCID 167693TrimethylsilyldiazomethaneHCID 219302Oxane-4-carboxylic acid

Product 1

HCID 131972252-Bromo-1-(oxan-4-yl)ethan-1-one

Sources & evidence

ORD record
ord-bf170af331c14324ae9d44895dbebf8d
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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