Water → 5,6-Dihydro-4-oxo-5-(2-ethoxycarbonylethyl)thieno[2,3-b]thiopyran

HRID 951684Notes

Reaction equation

HRID 951684 reaction equation
[CH2:34]([Cl:35])[Cl:36].[Cl:23][Sn:24]([Cl:25])([Cl:26])[Cl:27].[O:29]=[CH:30][N:31]([CH3:32])[CH3:33].[OH2:28].[S:1]([Cl:2])([Cl:3])=[O:4].[s:5]1[c:6]([S:10][CH2:11][CH:12]([C:13](=[O:14])[OH:15])[CH2:16][CH2:17][C:18](=[O:19])[O:20][CH2:21][CH3:22])[cH:7][cH:8][cH:9]1>>[s:5]1[c:6]2[c:7]([cH:8][cH:9]1)[C:13](=[O:15])[CH:12]([CH2:16][CH2:17][C:18](=[O:19])[O:20][CH2:21][CH3:22])[CH2:11][S:10]2

Participants

7

Reactant 6

HCID 962WaterHCID 6228DimethylformamideHCID 6344DichloromethaneHCID 24287Tin tetrachlorideHCID 24386Thionyl ChlorideHCID 19745039HCID 19745039, compound

Product 1

HCID 678831665,6-Dihydro-4-oxo-5-(2-ethoxycarbonylethyl)thieno[2,3-b]thiopyran

Sources & evidence

ORD record
ord-32e5b49997ba4c51944e8dae7b1e3ce0
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

Loading…