Dichloromethane → Tert-butyl 4-(2,2-dibromovinyl)piperidine-1-carboxylate

HRID 952835Notes

Reaction equation

HRID 952835 reaction equation
[Br:20][C:21]([Br:22])([Br:23])[Br:24].[C:32]([CH3:33])([CH3:34])([CH3:35])[O:36][C:37](=[O:38])[N:39]1[CH2:40][CH2:41][CH:42]([CH:45]=[O:46])[CH2:43][CH2:44]1.[CH3:25][CH2:26][N:27]([CH2:28][CH3:29])[CH2:30][CH3:31].[Cl:47][CH2:48][Cl:49].[c:1]1([P:2]([c:3]2[cH:4][cH:5][cH:6][cH:7][cH:8]2)[c:9]2[cH:10][cH:11][cH:12][cH:13][cH:14]2)[cH:15][cH:16][cH:17][cH:18][cH:19]1>>[Br:20][C:21]([Br:24])=[CH:45][CH:42]1[CH2:41][CH2:40][N:39]([C:37]([O:36][C:32]([CH3:33])([CH3:34])[CH3:35])=[O:38])[CH2:44][CH2:43]1

Participants

6

Reactant 5

HCID 6344DichloromethaneHCID 8471TriethylamineHCID 11205Carbon tetrabromideHCID 11776TriphenylphosphineHCID 1514430tert-Butyl 4-formylpiperidine-1-carboxylate

Product 1

HCID 11474132Tert-butyl 4-(2,2-dibromovinyl)piperidine-1-carboxylate

Sources & evidence

ORD record
ord-d152c854e8284ba8ae2132f3ccfd83df
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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