Dichloromethane → tert-butyl 7-(methanesulfonamido)-6,10-dioxo-2,3,4,7,8,9-hexahydro-1H-pyridazino[1,2-a]diazepine-4-carboxylate

HRID 953771Notes

Reaction equation

HRID 953771 reaction equation
[CH3:31][S:32]([Cl:33])(=[O:34])=[O:35].[CH3:39][CH2:40][O:41][C:42]([CH3:43])=[O:44].[CH:22]([N:23]([CH:24]([CH3:25])[CH3:26])[CH2:27][CH3:28])([CH3:29])[CH3:30].[Cl:36][CH2:37][Cl:38].[NH2:1][CH:2]1[CH2:3][CH2:4][C:5](=[O:21])[N:6]2[N:7]([C:8]1=[O:9])[CH:10]([C:14](=[O:15])[O:16][C:17]([CH3:18])([CH3:19])[CH3:20])[CH2:11][CH2:12][CH2:13]2>>[NH:1]([CH:2]1[CH2:3][CH2:4][C:5](=[O:21])[N:6]2[N:7]([C:8]1=[O:9])[CH:10]([C:14](=[O:15])[O:16][C:17]([CH3:18])([CH3:19])[CH3:20])[CH2:11][CH2:12][CH2:13]2)[S:32]([CH3:31])(=[O:34])=[O:35]

Participants

6

Reactant 5

HCID 6344DichloromethaneHCID 8857Ethyl AcetateHCID 31297Methanesulfonyl chlorideHCID 81531DiisopropylethylamineHCID 11174000HCID 11174000, compound

Product 1

HCID 18465701tert-butyl 7-(methanesulfonamido)-6,10-dioxo-2,3,4,7,8,9-hexahydro-1H-pyridazino[1,2-a]diazepine-4-carboxylate

Sources & evidence

ORD record
ord-31df1a08ad334ecc9c3a9fc9d4a7b96f
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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