Methanol → Methyl 3-acetylamino-6-bromo-2-nitrobenzoate

HRID 961291Notes

Reaction equation

HRID 961291 reaction equation
[C:1]([CH3:2])(=[O:3])[NH:4][c:5]1[c:6]([N+:15](=[O:16])[O-:17])[c:7]([C:8](=[O:9])[OH:10])[c:11]([Br:14])[cH:12][cH:13]1.[CH2:31]1[O:32][CH2:33][CH2:34][CH2:35]1.[CH3:18][Si:19]([CH:20]=[N+:21]=[N-:22])([CH3:23])[CH3:24].[CH3:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30].[CH3:36][OH:37]>>[C:1]([CH3:2])(=[O:3])[NH:4][c:5]1[c:6]([N+:15](=[O:16])[O-:17])[c:7]([C:8]([O:9][CH3:18])=[O:10])[c:11]([Br:14])[cH:12][cH:13]1

Participants

6

Reactant 5

HCID 887MethanolHCID 8028TetrahydrofuranHCID 8058HexaneHCID 167693TrimethylsilyldiazomethaneHCID 114039033-Acetylamino-6-bromo-2-nitro-benzoic acid

Product 1

HCID 11151255Methyl 3-acetylamino-6-bromo-2-nitrobenzoate

Sources & evidence

ORD record
ord-fcddcc19aae245ff8f0182ccf172a7b9
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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