→ HCID 11379804, compound

HRID 962318Notes

Reaction equation

HRID 962318 reaction equation
CC(=O)O.CCCCCC=O.CCO.CCOC(=O)CC(C)=O.NC(N)=O.O.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CCCCCC1NC(=O)NC(C)=C1C(=O)OCC

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 11379804HCID 11379804, compoundYield 35%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 702EthanolOtherHCID 1176UreaOtherHCID 6184HexanalOtherHCID 8868Ethyl AcetoacetateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-8f4798b8fde74de885d7e98a40d4ab6d
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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