→ HCID 3093021, compound

HRID 962328Notes

Reaction equation

HRID 962328 reaction equation
CC(=O)CC(=O)OC(C)C.CCO.NC(N)=O.O.O=Cc1cccc([N+](=O)[O-])c1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CC1=C(C(=O)OC(C)C)C(c2cccc([N+](=O)[O-])c2)NC(=O)N1

Participants

6

Reactant 0

No Reactant data yet.

Product 1

HCID 3093021HCID 3093021, compoundYield 73%

Reagents, catalysts & solvents 5

HCID 702EthanolOther2×HCID 1176UreaOtherHCID 74493-NitrobenzaldehydeOtherHCID 68329Isopropyl acetoacetateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-92ea9154208b4cf8a3f36e999926a4f9
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

Loading…