→ HCID 4485966, compound

HRID 962330Notes

Reaction equation

HRID 962330 reaction equation
CC(=O)CC(=O)OC(C)(C)C.CCO.NC(N)=O.O.O=Cc1ccccc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CC1=C(C(=O)OC(C)(C)C)C(c2ccccc2)NC(=O)N1

Participants

6

Reactant 0

No Reactant data yet.

Product 1

HCID 4485966HCID 4485966, compoundYield 49%

Reagents, catalysts & solvents 5

HCID 240BenzaldehydeOtherHCID 702EthanolOther2×HCID 1176UreaOtherHCID 15538Tert-butyl acetoacetateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-d6d009e97ad7484cb7e7ff8018cbbe1b
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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