→ HCID 10752818, compound

HRID 962333Notes

Reaction equation

HRID 962333 reaction equation
CC(=O)CC(C)=O.CCO.Cc1cccc(C=O)c1.NC(N)=O.O.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CC(=O)C1=C(C)NC(=O)NC1c1cccc(C)c1

Participants

6

Reactant 0

No Reactant data yet.

Product 1

HCID 10752818HCID 10752818, compoundYield 68%

Reagents, catalysts & solvents 5

HCID 702EthanolOther2×HCID 1176UreaOtherHCID 121053-MethylbenzaldehydeOtherHCID 31261AcetylacetoneOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-41e65d15855746959fe135994788aea4
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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