→ HCID 110273791, compound

HRID 962337Notes

Reaction equation

HRID 962337 reaction equation
CC(=O)O.CCO.COCC(=O)CC(=O)OC.NC(N)=O.O.O=Cc1cccc([N+](=O)[O-])c1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>COCC1=C(C(=O)OC)C(c2cccc([N+](=O)[O-])c2)NC(=O)N1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 110273791HCID 110273791, compoundYield 35%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 702EthanolOtherHCID 1176UreaOtherHCID 74493-NitrobenzaldehydeOtherHCID 123500Methyl 4-methoxyacetoacetateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-c41b9a539b19471e89b987cf573d9da6
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

Loading…