→ HCID 2860103, compound

HRID 962340Notes

Reaction equation

HRID 962340 reaction equation
CCCC(=O)CC(=O)OCC.CCO.NC(N)=O.O.O=Cc1ccc([N+](=O)[O-])cc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CCCC1=C(C(=O)OCC)C(c2ccc([N+](=O)[O-])cc2)NC(=O)N1

Participants

6

Reactant 0

No Reactant data yet.

Product 1

HCID 2860103HCID 2860103, compoundYield 41%

Reagents, catalysts & solvents 5

HCID 5414-NitrobenzaldehydeOtherHCID 702EthanolOther2×HCID 1176UreaOtherHCID 238498Ethyl 3-oxohexanoateOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-fbd04a97510849a898adcad701e2bb44
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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