→ HCID 4208966, compound

HRID 962346Notes

Reaction equation

HRID 962346 reaction equation
CC(=O)CC(=O)Nc1ccccc1.CC(=O)O.CCO.NC(N)=O.O.O=Cc1ccccc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CC1=C(C(=O)Nc2ccccc2)C(c2ccccc2)NC(=O)N1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 4208966HCID 4208966, compoundYield 55%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 240BenzaldehydeOtherHCID 702EthanolOtherHCID 1176UreaOtherHCID 7592AcetoacetanilideOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-e15a2253fa1840b59194ce7d78b3d998
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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