→ HCID 3152072, compound

HRID 962347Notes

Reaction equation

HRID 962347 reaction equation
C1COCCO1.CC(=O)CC(=O)Nc1ccccc1.CCO.COc1cc(C=O)ccc1O.NC(N)=O.[Cl-].[H+]>>COc1cc(C2NC(=O)NC(C)=C2C(=O)Nc2ccccc2)ccc1O

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 3152072HCID 3152072, compoundYield 28%

Reagents, catalysts & solvents 6

HCID 702EthanolOther2×HCID 1176UreaOtherHCID 1183VanillinOtherHCID 7592AcetoacetanilideOtherHCID 312751,4-DioxaneOtherHCID 183483317647-01-0Other

Conditions

Temperature
100 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-a3de4381e09f4cb39e164eeee914f164
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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