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HRID9724

反应详情

EQUATION

反应方程式

HRID 9724 的结构方程式

REACTANTS

反应物

3
结构：O
HCID962

Water

H2O

结构：CC(C)(N)CO
HCID11807

2-Amino-2-methylpropan-1-ol

C4H11NO

结构：O=C1OC(=O)c2cc([N+](=O)[O-])ccc21
HCID230976

4-Nitrophthalic anhydride

C8H3NO5

PRODUCTS

生成物

1
结构：CC(C)(CO)N1Cc2ccc([N+](=O)[O-])cc2C1
HCID21988156

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

20 g of 4-Nitro-phthalic anhydride and 8.94 g of 2-amino-2-methylpropanol were heated to 170° C. for 30 min. After cooling, water and CH2Cl2 were added, and the organic phase separated, concentrated and purified by chromatography on silica (eluent CH2Cl2/MeOH 97/3).

WORKUP

后处理

  1. temperatureAfter cooling
  2. customthe organic phase separated
  3. concentrationconcentrated
  4. custompurified by chromatography on silica (eluent CH2Cl2/MeOH 97/3)