Furfurylamine → HCID 21405563, compound

HRID 972824Notes

Reaction equation

[CH2:1]([NH2:7])[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[C:8]([O:12][CH3:13])(=[O:11])[CH:9]=[CH2:10]>>[CH3:13][O:12][C:8]([CH2:9][CH2:10][N:7]([CH2:1][C:2]1[O:6][CH:5]=[CH:4][CH:3]=1)[CH2:10][CH2:9][C:8]([O:12][CH3:13])=[O:11])=[O:11]

Participants

Reactant 2

HCID 3438Furfurylamine

HCID 7294Methyl Acrylate

Product 1

HCID 21405563HCID 21405563, compound

Procedure

48.56 Grams of furfurylamine and 200 milliliters of methyl acrylate are refluxed together for 84 hours. The excess methyl acrylate is evaporated off to give 133.46 grams of N,N-di(2-methoxycarbonylethyl)furfurylamine.

Workup

customThe excess methyl acrylate is evaporated off

Sources & evidence

ORD record: ord-7a9467539d4d4751b8dc31ca08e55248
Source dataset: uspto-grants-1977_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04053615

Reaction notes

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