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HRID973809

反应详情

EQUATION

反应方程式

HRID 973809 的结构方程式

REACTANTS

反应物

3
反应SMILES：O
HCID962

Water

H2O

反应SMILES：C1CCOC1
HCID8028

Tetrahydrofuran

C4H8O

反应SMILES：O=C(Cl)c1ccc(-c2nc(C(Cl)(Cl)Cl)nc(C(Cl)(Cl)Cl)n2)cc1
HCID14473251

未命名化合物

PRODUCTS

产物

1
反应SMILES：O=C(O)c1ccc(-c2nc(C(Cl)(Cl)Cl)nc(C(Cl)(Cl)Cl)n2)cc1
HCID14572915

4-[4,6-Bis(trichloromethyl)-1,3,5-triazin-2-yl]benzoic acid

C12H5Cl6N3O2

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

4-(4,6-Bis(trichloromethyl)-s-triazin-2-yl)-benzoyl chloride pw) is added to a mixture of tetrahydrofuran (10 pw) and water (5 pw). To complete the reaction, 1 pw of triethylamine is added after 6 minutes, and the mixture is stirred for another 10 minutes. The solvent is removed by distillation, and the residue is recrystallized from toluene/benzine. The product is identical with the compounds described in Examples 12 and 16.

WORKUP

后处理

  1. additionis added after 6 minutes
  2. customThe solvent is removed by distillation
  3. customthe residue is recrystallized from toluene/benzine