Phenethylamine → HCID 15924278, compound

HRID 974256Notes

Reaction equation

HRID 974256 reaction equation
[C:1]([CH2:6][CH2:7][CH:8]1[C:13](=O)[CH2:12][CH2:11][CH2:10][C:9]1=[O:15])([O:3]CC)=O.[C:16]1([CH2:22][CH2:23][NH2:24])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1.C1(C)C(C)=CC=CC=1>O>[C:16]1([CH2:22][CH2:23][N:24]2[C:13]3[CH2:12][CH2:11][CH2:10][C:9](=[O:15])[C:8]=3[CH2:7][CH2:6][C:1]2=[O:3])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

5

Reactant 3

HCID 1001PhenethylamineHCID 7237O-XyleneHCID 11745931HCID 11745931, compound

Product 1

HCID 15924278HCID 15924278, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Prepared analogously to Example 27 from 2-(2-carbethoxy-ethyl)-cyclohexan-1,3-dione and 2-phenylethylamine in boiling xylene using a water separator.

Sources & evidence

ORD record
ord-2cde438ab5d348668f16c50eca61f8f2
Source dataset
uspto-grants-1991_11
Patent number
US05068334

Reaction notes

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