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HRID977099

反应详情

EQUATION

反应方程式

HRID 977099 的结构方程式

REACTANTS

反应物

1
结构：CCOC(=O)c1sc(-c2ccc(Cl)c([N+](=O)[O-])c2)nc1C
HCID19965170

Ethyl 2-(4-chloro-3-nitrophenyl)-4-methyl-5-thiazolecarboxylate

C13H11ClN2O4S

PRODUCTS

生成物

1
结构：Cc1ncsc1C(=O)O
HCID209805

5-Thiazolecarboxylic acid, 4-methyl-

C5H5NO2S

收率 56%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCNCC
溶剂HCID8021

Diethylamine

C4H11N

PROCEDURE

实验过程

Ethyl 2-(4-chloro-3-nitrophenyl)-4-methyl-5-thiazolecarboxylate in diethylamine was heated in the same manner as that of Example 35 and hydrolyzed to give 2-(4-N,N-diethylamino)-3-nitrophenyl)-4-methyl-5-thiazolecarboxylic acid (yield: 56%).