Hydrazine hydrate (1:1) → HCID 86741510, compound

HRID 979031Notes

Reaction equation

HRID 979031 reaction equation
[NH:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[O:11][C:9](=[O:10])[C:8](=[C:12]=[O:13])[CH2:7]1.O.[NH2:15][NH2:16]>C(O)C>[OH2:10].[NH:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[O:11][C:9](=[N:15][NH2:16])[C:8](=[C:12]=[O:13])[CH2:7]1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 86741512HCID 86741512, compound

Product 1

HCID 86741510HCID 86741510, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

7.2 g (0.04 mol) of 4-(2-pyrrolyl)-carbonyl-γ-butyrolactone and 2.5 ml (0.05 mol) of hydrazine hydrate are stirred in ethanol at room temperature for 4 hours. The product which has crystallised out is filtered off with suction and rinsed with ethanol.

Workup

  1. customThe product which has crystallised out
  2. filtrationis filtered off with suction
  3. washrinsed with ethanol

Sources & evidence

ORD record
ord-50c377cf8a34415cac5663574a2acd94
Source dataset
uspto-grants-1987_05
Patent number
US04666902

Reaction notes

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