Dodecylamine → HCID 13361730, compound

HRID 985966Notes

Reaction equation

HRID 985966 reaction equation
O=[CH:2][C@@H:3]([C@H:5]([C@@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:13]([NH2:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>C(O)C>[CH2:13]([NH:25][C@@H:2]1[O:10][C@H:9]([CH2:11][OH:12])[C@@H:7]([OH:8])[C@H:5]([OH:6])[C@H:3]1[OH:4])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

4

Reactant 2

HCID 13583DodecylamineHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal

Product 1

HCID 13361730HCID 13361730, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

18 g of glucose were stirred in 50 ml of ethanol at 70° C., 18.5 g of dodecylamine were then added, the mixture was heated again until a clear solution was obtained, the solution was allowed to cool to room temperature and, after 20 hours, the crystals which had precipitated were filtered off with suction. The product was washed with ethanol and ether and dried in vacuo.

Workup

  1. temperaturethe mixture was heated again until a clear solution
  2. customwas obtained
  3. customthe crystals which had precipitated
  4. filtrationwere filtered off with suction
  5. washThe product was washed with ethanol and ether
  6. customdried in vacuo

Sources & evidence

ORD record
ord-94df5f7afcbe498fb9cdecc1eb1bb5a6
Source dataset
uspto-grants-1987_12
Patent number
US04710491

Reaction notes

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