Dodecylamine → HCID 70445007, compound

HRID 985978Notes

Reaction equation

HRID 985978 reaction equation
[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:14].O[CH:16]1[O:24][C@H:23]([CH2:25][OH:26])[C@@H:21]([OH:22])[C@H:19]([OH:20])[C@H:17]1[NH2:18]>>[ClH:14].[CH2:1]([NH:13][CH:16]1[O:24][C@H:23]([CH2:25][OH:26])[C@@H:21]([OH:22])[C@H:19]([OH:20])[C@H:17]1[NH2:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 13583DodecylamineHCID 2723635(3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride

Product 1

HCID 70445007HCID 70445007, compound

Procedure

46 g of dodecylamine were melted at 60° and 31 g of glucosamine hydrochloride were added, with stirring. After cooling to room temperature, the product precipitated. The solid was extracted three times by stirring with ether and filtered off with suction and then dried under a high vacuum.

Workup

  1. additionwere added
  2. customthe product precipitated
  3. extractionThe solid was extracted three times
  4. stirringby stirring with ether
  5. filtrationfiltered off with suction
  6. customdried under a high vacuum

Sources & evidence

ORD record
ord-9294e126bd8b47b9b7be998f2dfcd389
Source dataset
uspto-grants-1987_12
Patent number
US04710491

Reaction notes

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