Barium bis(2-ethylhexanoate) → Barium bis(2-ethylhexanoate)

HRID 986880Notes

Reaction equation

HRID 986880 reaction equation
[O-2:1].[O-2].[O-2].[Al+3:4].[Al+3].[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7].[Ba+2:16].[CH2:17]([CH:19]([CH2:23][CH2:24][CH2:25][CH3:26])[C:20]([O-:22])=[O:21])[CH3:18]>C1(C)C=CC=CC=1>[Ba:16].[O-2:10].[O-2:21].[O-2:1].[Al+3:4].[Al+3:4].[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7].[Ba+2:16].[CH2:17]([CH:19]([CH2:23][CH2:24][CH2:25][CH3:26])[C:20]([O-:22])=[O:21])[CH3:18]

Participants

6

Reactant 2

HCID 102821Barium bis(2-ethylhexanoate)HCID 9989226Alumina

Product 3

HCID 102821Barium bis(2-ethylhexanoate)HCID 5355457BariumHCID 9989226Alumina

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Barium coated alpha alumina was prepared by adding 5,000 g of Alcoa A16-SG alpha alumina to a 2 liter solution of 6 wt % barium 2-ethylhexanoate in toluene. The mixture was stirred for 20 minutes. The liquid was filtered off leaving alpha alumina particles with a thin coating of barium 2-ethylhexanoate. The particles were then calcined to 500° C. for 1 hour.

Workup

  1. filtrationThe liquid was filtered off

Sources & evidence

ORD record
ord-9bf2715c5a4844c49bf7a5c23634deac
Source dataset
uspto-grants-2003_10
Patent number
US06630062B1

Reaction notes

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