HRID987586

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID971

Oxalic acid

C2H2O4

HCID1923

8-Hydroxyquinoline

C9H7NO

HCID18009170

6-Methoxyquinolin-8-ol

C10H9NO2

PRODUCTS

生成物

结构：c1ccc2cc(C3CC4CCC(C3)N4CCOc3cccc4cccnc34)ccc2c1

HCID10201518

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The title compound is prepared according to Example 8, Step 5, except 8-hydroxyquinoline is used in place 6-methoxyquinolin-8-ol. The corresponding oxalate salt is prepared by treating the title compound with 1 equiv. oxalic acid in DMF to precipitate a white solid. Yield: 51%; mp: 110-113° C.; MS (ES) m/z: 409 (MH)+.

WORKUP

后处理

customThe title compound is prepared
customto precipitate a white solid