HRID988914

反应详情

EQUATION

反应方程式

HRID 988914 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
50 °C

PROCEDURE

实验过程

A mixture of 98.1 g (0.5 mol) of N-[2-hydroxy-4-nitrophenyl)acetamide and 69.2 g (0.5 mol) of potassium carbonate in 500ml of dimethylformamide was heated to 50° C. with stirring, 113.0 g (1 mol) of 1,3-dichloropropane were then added and heating was continued at 50° C. for one hour.

WORKUP

后处理

  1. temperatureheating