3-Hydroxybenzaldehyde → HCID 18004785, compound

HRID 988991Notes

Reaction equation

HRID 988991 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[C:8]([N+:12]#[C-:13])([CH3:11])([CH3:10])[CH3:9].[OH:14][C:15]1[CH:16]=[C:17]([CH:20]=[CH:21][CH:22]=1)[CH:18]=O>Cl(O)(=O)(=O)=O>[C:8]([NH:12][C:13]1[N:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]2=[N:1][C:18]=1[C:17]1[CH:16]=[C:15]([OH:14])[CH:22]=[CH:21][CH:20]=1)([CH3:11])([CH3:10])[CH3:9]

Participants

5

Reactant 3

HCID 1013-HydroxybenzaldehydeHCID 104392-AminopyridineHCID 23577Tert-Butyl isocyanide

Product 1

HCID 18004785HCID 18004785, compound

Reagents, catalysts & solvents 1

HCID 24247Perchloric AcidSolvent

Procedure

Compound (10) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyridine solution (0.1 M, MC), 0.575 ml tert-butylisonitrile solution (0.2 M, MC), 0.500 ml 3-hydroxybenzaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%).

Sources & evidence

ORD record
ord-31727647e13443bbb6a428cd6fe8030e
Source dataset
uspto-grants-2003_10
Patent number
US06638933B2

Reaction notes

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