Trifluoromethanesulfonic acid → HCID 11000413, compound

HRID 989063Notes

Reaction equation

HRID 989063 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([F:8])[N:3]=1.[F:9][C:10]([F:16])([F:15])[S:11]([OH:14])(=[O:13])=[O:12]>>[F:9][C:10]([F:16])([F:15])[S:11]([O-:14])(=[O:13])=[O:12].[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([F:8])[N+:3]=1[CH3:10]

Participants

3

Reactant 2

HCID 62406Trifluoromethanesulfonic acidHCID 739342,6-Difluoropyridine

Product 1

HCID 11000413HCID 11000413, compound

Procedure

10 mmol of 2,6-difluoropyridine and 10 mmol of trifluoromethanesulphonic acid are mixed in a 50 ml round-bottomed flask and the mixture is stirred for 1 hour at ambient temperature under a nitrogen atmosphere. The white solid obtained is used directly in the following reaction without further purification.

Workup

  1. customThe white solid obtained
  2. customis used directly in the following reaction without further purification

Sources & evidence

ORD record
ord-3ee4d5791f7e48af8ab0a8dd5bfcab3d
Source dataset
uspto-grants-2003_10
Patent number
US06638946B2

Reaction notes

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