Ethylene carbonate → HCID 15671420, compound

HRID 991647Notes

Reaction equation

HRID 991647 reaction equation
[C:1]1([C:7]2[CH:8]=[C:9]([OH:13])[CH:10]=[CH:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(=O)O[CH2:17][CH2:16][O:15]1>CN(C=O)C>[C:1]1([C:7]2[CH:8]=[C:9]([CH:10]=[CH:11][CH:12]=2)[O:13][CH2:17][CH2:16][OH:15])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 7303Ethylene carbonateHCID 113813-Phenylphenol

Product 1

HCID 15671420HCID 15671420, compoundYield 86%

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

The title compound was prepared according to the procedure of Example 114, Step 1 starting from 3-phenylphenol (1.72 g, 10.1 mmol) and ethylene carbonate (0.80 g, 9.1 mmol) and DMF (3 mL). Semi-solid; yield 86%. MS m/z 214 (M)+.

Sources & evidence

ORD record
ord-bc837dadc9764555a64d3a05378fb645
Source dataset
uspto-grants-2002_10
Patent number
US06465467B1

Reaction notes

Loading…