Acetic Acid → HCID 74019072, Verbindung

HRID 1175799

Reaktionsgleichung

Reaktionsgleichung von HRID 1175799
Cl.[CH3:2][O:3][C:4]1[CH:5]=[C:6]([NH:10][NH2:11])[CH:7]=[CH:8][CH:9]=1.[N+:12]([CH2:15][C:16]([C:18]1C=CC=C[CH:19]=1)=O)([O-:14])=[O:13].[C:24]([O-])(=O)[CH3:25].[Na+].[C:29](O)(=O)[CH3:30]>O>[CH3:2][O:3][C:4]1[CH:5]=[C:6]([NH:10][N:11]=[C:29]([C:24]2[CH:25]=[CH:19][CH:18]=[CH:16][C:15]=2[N+:12]([O-:14])=[O:13])[CH3:30])[CH:7]=[CH:8][CH:9]=1

Komponenten

6

Edukt 4

HCID 176Acetic AcidHCID 948332-Nitro-1-phenylethanoneHCID 517045Sodium AcetateHCID 27239403-Methoxyphenylhydrazine hydrochloride

Produkt 1

HCID 74019072HCID 74019072, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

A mixture of 3-methoxyphenylhydrazine hydrochloride (1.75 g), 2-nitroacetophenone (1.65 g), sodium acetate (0.82 g) and acetic acid (10 ml) was stirred at room temperature for 4 days. To the reaction mixture was added water, extracted with ethyl acetate. The extract was washed with water, brine, dried over anhydrous magnesium sulfate. The solvent was distilled off under reduced pressure to obtain the target compound (2.72 g).

Aufarbeitung

  1. extractionextracted with ethyl acetate
  2. washThe extract was washed with water, brine
  3. dry with materialdried over anhydrous magnesium sulfate
  4. distillationThe solvent was distilled off under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-573261e1a46940b09dc4e699d60da9d2
Quelldatensatz
uspto-grants-2010_11
Patentnummer
US07842701B2

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