2,3-Dihydroxybutanedioic Acid → Dilithium tartrate
Reaktionsgleichung
[C:1]([OH:10])(=[O:9])[CH:2]([CH:4]([C:6]([OH:8])=[O:7])[OH:5])[OH:3].[OH-].[Li+:12]>O>[C:1]([O-:10])(=[O:9])[CH:2]([CH:4]([C:6]([O-:8])=[O:7])[OH:5])[OH:3].[Li+:12].[Li+:12]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Tartaric acid (15.0 g, 0.1 mole) is dissolved in 40 ml. water and treated with lithium hydroxide (8.4 g, 0.2 mole). The resulting solution is evaporated to a small volume under reduced pressure and the residue is treated with p-dioxane. The resulting precipitate is filtered and dried under vacuum to give the di-lithium tartarate (17.7 g).
Aufarbeitung
- customThe resulting solution is evaporated to a small volume under reduced pressure
- additionthe residue is treated with p-dioxane
- filtrationThe resulting precipitate is filtered
- customdried under vacuum
Quellen und Nachweise
- ORD-Eintrag
- ord-a67d48d9e9d04959beeeb614c22e22ee
- Quelldatensatz
- uspto-grants-1980_06
- Patentnummer
- US04206219
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