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Hydrochloric Acid → 1-{[1-(1-Ethyl-propyl)-2-thiophen-2-ylmethyl-1H-benzimidazole-5-carbonyl]-amino}-cycloheptanecarboxylic acid methyl ester

HRID 1750163
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Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 1750163
[CH2:1]([CH:3]([N:6]1[C:10]2[CH:11]=[CH:12][C:13]([C:15](O)=[O:16])=[CH:14][C:9]=2[N:8]=[C:7]1[CH2:18][C:19]1[S:20][CH:21]=[CH:22][CH:23]=1)[CH2:4][CH3:5])[CH3:2].C1C=NC2N(O)N=NC=2C=1.CCN(C(C)C)C(C)C.Cl.[NH2:44][C:45]1([C:52]([O:54][CH3:55])=[O:53])[CH2:51][CH2:50][CH2:49][CH2:48][CH2:47][CH2:46]1.Cl>CN(C=O)C.O.C(Cl)CCl>[CH3:55][O:54][C:52]([C:45]1([NH:44][C:15]([C:13]2[CH:12]=[CH:11][C:10]3[N:6]([CH:3]([CH2:1][CH3:2])[CH2:4][CH3:5])[C:7]([CH2:18][C:19]4[S:20][CH:21]=[CH:22][CH:23]=4)=[N:8][C:9]=3[CH:14]=2)=[O:16])[CH2:51][CH2:50][CH2:49][CH2:48][CH2:47][CH2:46]1)=[O:53]
KomponentenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion

Komponenten

9

Edukt 5

HCID 313Hydrochloric AcidHCID 81531Diisopropylethylamine2×HCID 181649HOAtHCID 42614177Methyl 1-aminocycloheptane-1-carboxylate hydrochlorideHCID 867143731-(1-ethyl-propyl)-2-thiophen-2-ylmethyl-1H-benzoimidazole-5-carboxylic acid

Produkt 1

HCID 86714372
1-{[1-(1-Ethyl-propyl)-2-thiophen-2-ylmethyl-1H-benzimidazole-5-carbonyl]-amino}-cycloheptanecarboxylic acid methyl ester
Ausbeute 86,2 %

Reagenzien, Katalysatoren, Lösungsmittel 3

HCID 111,2-DichloroethaneLösungsmittelHCID 962WaterLösungsmittelHCID 6228DimethylformamideLösungsmittel

Versuchsvorschrift

To a solution of 160 mg of 1-(1-ethyl-propyl)-2-thiophen-2-ylmethyl-1H-benzoimidazole-5-carboxylic acid (The preparation of intermediates is described below) in 3 ml of dry DMF 73 mg of HOAT, 131 mg of EDC and 0.16 ml of DIPEA were added at 0° C. After 15 min 100 mg of methyl 1-amino-cycloheptanecarboxylate-hydrochloride and 0.16 ml of DIPEA were added and the reaction was stirred at it for 16 h. The reaction was then poured into water and the pH was adjusted to 3 by the addition of 2 M aqueous hydrochloric acid. The reaction was extracted with ethyl acetate three times. The combined organic phases were washed with saturated aqueous sodium bicarbonate solution and brine, dried over magnesium sulphate and concentrated. The crude product was purified by HPLC to yield 200 mg (85%) of 1-{[1-(1-Ethyl-propyl)-2-thiophen-2-ylmethyl-1H-benzimidazole-5-carbonyl]-amino}-cycloheptanecarboxylic acid methyl ester.

Aufarbeitung

  1. additionwere added at 0° C
  2. extractionThe reaction was extracted with ethyl acetate three times
  3. washThe combined organic phases were washed with saturated aqueous sodium bicarbonate solution and brine
  4. dry with materialdried over magnesium sulphate
  5. concentrationconcentrated
  6. customThe crude product was purified by HPLC

Quellen und Nachweise

ORD-Eintrag
ord-58c2a66162b94c7d830468af5a8c3aae
Quelldatensatz
uspto-grants-2015_10
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US09156796B2

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