Nitric Acid → 4-Tert-butyl-1-methyl-2-nitrobenzene

HRID 23493

Reaktionsgleichung

Reaktionsgleichung von HRID 23493
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].OS(O)(=O)=O.[N+:17]([O-])([OH:19])=[O:18]>O>[C:1]([C:5]1[CH:6]=[CH:7][C:8]([CH3:11])=[C:9]([N+:17]([O-:19])=[O:18])[CH:10]=1)([CH3:4])([CH3:3])[CH3:2]

Komponenten

5

Edukt 3

HCID 944Nitric AcidHCID 1118Sulfuric AcidHCID 73904-tert-Butyltoluene

Produkt 1

HCID 109544154-Tert-butyl-1-methyl-2-nitrobenzene

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Nitration was performed as described in General Method 12 using tert-butyl-4-methylbenzene (25 g), concentrated H2SO4 (92 g), 70% HNO3 (82 g), and H2O (25 g). The crude product was purified via distillation under vacuum.

Aufarbeitung

  1. distillationThe crude product was purified via distillation under vacuum

Quellen und Nachweise

ORD-Eintrag
ord-28047e1787ec4cb588412d11eb80d13c
Quelldatensatz
uspto-grants-2005_02
Patentnummer
US06852711B2

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