Reaktionsgleichung
[C:1]1(=[O:6])[O:5][CH2:4][CH2:3][O:2]1>B([O-])=O.[Na+].C(O)COCCO>[C:1]1(=[O:6])[O:5][CH2:4][CH2:3][O:2]1.[C:1](=[O:5])=[O:2]Komponenten
5
Edukt 1
Produkt 2
Reagenzien, Katalysatoren, Lösungsmittel 2
Reaktionsbedingungen
- Temperatur
- 160 °C
Versuchsvorschrift
A 50:1 mole ratio of ethylene carbonate to diethylene glycol is heated with stirring under a nitrogen atmosphere for 45 hours at 160° C. using 1.0 percent sodium metaborate as catalyst to give 100 percent ethylene carbonate conversion to a poly(alkylene carbonate) polyol with 17.8 percent carbon dioxide. The catalyst is removed as in Example 1.
Quellen und Nachweise
- ORD-Eintrag
- ord-ebfbf94f624d48f287be4b52346279fa
- Quelldatensatz
- uspto-grants-1987_11
- Patentnummer
- US04709069
Verknüpfte Notizen
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