1-Methylimidazole → HCID 178448538, Verbindung
Reaktionsgleichung
[Cl:1][CH2:2][CH2:3][CH2:4][CH3:5].[CH3:6][N:7]1[CH:11]=[CH:10][N:9]=[CH:8]1>>[Cl-:1].[CH2:2]([N+:9]1[CH:10]=[CH:11][N:7]([CH3:6])[CH:8]=1)[CH2:3][CH2:4][CH3:5]Komponenten
3
Reaktionsbedingungen
- Temperatur
- 60 °C
Versuchsvorschrift
251.4 g of 1-chlorobutane (2.7 mol) are loaded into a 1 l glass reactor. The mixture is heated to 60° C., and then 148.6 g of 1-methylimidazole (1.8 mol) are poured in dropwise, with stirring. The mixture is left to react for 24 h at 80° C. The reaction mixture is evaporated under vacuum. 309 g of 1-butyl-3-methylimidazolium chloride are obtained in the form of a yellowish solid (yield=98%). The product is used as it is without further purification.
Aufarbeitung
- waitThe mixture is left
- customto react for 24 h at 80° C
- customThe reaction mixture is evaporated under vacuum
Quellen und Nachweise
- ORD-Eintrag
- ord-68bc9c3131dd4c65bf273fb78a69005b
- Quelldatensatz
- uspto-grants-2004_03
- Patentnummer
- US06700007B2
Notizen zur Reaktion
Wird geladen…