Acetic Acid → Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

HRID 972462

Reaktionsgleichung

Reaktionsgleichung von HRID 972462
[C:1](O)(=O)C.[N:5]1[C:12]([NH2:13])=[N:11][C:9]([NH2:10])=[N:8][C:6]=1[NH2:7]>[NH4+].[O-][Mo]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O.O>[CH4:1].[C:6]1([NH2:7])[N:8]=[C:9]([NH2:10])[N:11]=[C:12]([NH2:13])[N:5]=1.[C:6]1([NH2:7])[N:8]=[C:9]([NH2:10])[N:11]=[C:12]([NH2:13])[N:5]=1

Komponenten

5

Edukt 2

HCID 176Acetic Acid2×HCID 7955Melamine

Produkt 1

HCID 103335Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 21895884Azanium bis(dioxido(dioxo)molybdenum)KatalysatorHCID 962WaterLösungsmittel3×

Versuchsvorschrift

Melamine molybdate was prepared in the presence of acetic acid as follows. 10 grams of melamine, 9.52 grams of acetic acid, and 250 ml water were dissolved together by refluxing in a 500 ml round-bottomed flask equipped with a stirrer and water-cooled condenser. 26.95 grams of ammonium dimolybdate was dissolved in 50 ml. hot water and then added to the first solution. A white precipitate formed immediately.

Aufarbeitung

  1. temperatureby refluxing in a 500 ml round-bottomed flask
  2. customequipped with a stirrer
  3. customA white precipitate formed immediately

Quellen und Nachweise

ORD-Eintrag
ord-f742670e27b647b1bf0c835b60db86de
Quelldatensatz
uspto-grants-1977_10
Patentnummer
US04053452

Verknüpfte Notizen

Wird geladen…