1-Phenylpiperazine → HCID 15636951, compound
Reaction equation
[NH2:1][CH2:2][CH2:3][N:4]1[CH2:7][CH2:6][CH2:5]1.[C:8](N1C=CN=C1)(N1C=CN=C1)=[O:9].[C:20]1([N:26]2[CH2:31][CH2:30][NH:29][CH2:28][CH2:27]2)[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>O1CCCC1>[C:20]1([N:26]2[CH2:31][CH2:30][N:29]([C:8]([NH:1][CH2:2][CH2:3][N:4]3[CH2:7][CH2:6][CH2:5]3)=[O:9])[CH2:28][CH2:27]2)[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
Following the procedure of Example 5, N-(2-aminoethyl)azetidine and 1,1'-carbonyldiimidazole are reacted together in tetrahydrofuran and the product thereof is reacted further with 1-phenylpiperazine to give the title compound.
Sources & evidence
- ORD record
- ord-c4e57128f04644ab99164ada8f999da5
- Source dataset
- uspto-grants-1990_10
- Patent number
- US04960776
Reaction notes
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