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Indole → 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

HRID 1490515
Notes
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Reaction equation

HRID 1490515 reaction equation
c1ccc2[nH]ccc2c1>C1CCOC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.Cc1cc(C)c(-n2ccn(-c3c(C)cc(C)cc3C)[c]2=[Ni]=[c]2n(-c3c(C)cc(C)cc3C)ccn2-c2c(C)cc(C)cc2C)c(C)c1>CC1(C)OB(c2c[nH]c3ccccc23)OC1(C)C
ParticipantsConditionsSources & evidenceReaction notes

Participants

5

Reactant 1

HCID 798Indole

Product 1

HCID 533980563-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indoleYield 65%

Reagents, catalysts & solvents 3

HCID 2733548Bis(pinacolato)diboraneReagentHCID 178425454HCID 178425454, compoundCatalystHCID 8028TetrahydrofuranSolvent

Conditions

Temperature
60 °C

Sources & evidence

ORD record
ord-ad55791473e2407489b2eb37793f2859
Source dataset
Borylation dataset from Roche
DOI
10.1021/jacs.0c05434

Reaction notes

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On this pageParticipantsConditionsSources & evidenceReaction notes