[NH2:1][C:2]1[CH:3]=[CH:4][C:5]([CH3:22])=[C:6]([NH:8][C:9]2[O:10][C:11]([C:14]3[CH:21]=[CH:20][C:17]([C:18]#[N:19])=[CH:16][CH:15]=3)=[CH:12][N:13]=2)[CH:7]=1.Cl[CH2:24][CH:25]=O.[BH3-]C#N.[Na+].C([O-])(O)=O.[Na+].[F:36][C:37]1[CH:42]=[CH:41][CH:40]=[C:39]([N:43]=[C:44]=[O:45])[CH:38]=1.CC(C)([O-])C.[K+]>C(#N)C.C1(C)C=CC=CC=1.O.C(OCC)(=O)C.C(O)(=O)C>[F:36][C:37]1[CH:38]=[C:39]([N:43]2[CH2:25][CH2:24][N:1]([C:2]3[CH:3]=[CH:4][C:5]([CH3:22])=[C:6]([NH:8][C:9]4[O:10][C:11]([C:14]5[CH:21]=[CH:20][C:17]([C:18]#[N:19])=[CH:16][CH:15]=5)=[CH:12][N:13]=4)[CH:7]=3)[C:44]2=[O:45])[CH:40]=[CH:41][CH:42]=1To a solution of 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile (558 mg, 2 mmol) and chloroacetaldehyde (50 wt. % in water, 628 mg, 4 mmol) in acetonitril (60 mL), was added at RT NaBH3CN (253 mg, 4 mmol) and dropwise acetic acid (0.4 mL). The mixture was stirred at room temperature 1 h. Ethyl acetate (50 mL) and saturated aqueous NaHCO3 (50 mL) were added. The organic layer was washed with brine (20 mL), dried over MgSO4 and concentrated to give a yellow solid. This was dissolved in toluene (40 mL) and treated with 1-Fluoro-3-isocyanato-benzene (274 mg, 2 mmol) at reflux for 2 h. After evaporation of solvent under reduced vacuum, the crude product was dissolved in isopropanol (60 mL) and treated with potassium tert-butoxide (1.8 g, 16 mmol) at RT for 5 h. Water (20 mL) was added, the organic layer was separated dried over MgSO4 and concentrated. The crude product was silica gel column chromatographed (dichloromethane/ethanol: 95/5) to give 408 mg (45%) of the title compound as a beige solid.
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