p-Toluidine → N-(4-methylphenyl)quinoxaline-6-carboxamide

Reaction equation

Cc1ccc(N)cc1.O=C(O)c1ccc2nccnc2c1.C1=CC=C(C=C1)P(=O)(C2=CC=CC=C2)OC3=C(C(=C(C(=C3F)F)F)F)F.CCN(C(C)C)C(C)C.CN(C)C=O>>Cc1ccc(NC(=O)c2ccc3nccnc3c2)cc1

addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

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addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

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