→ Ethyl 1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate
Reaction equation
CC(=O)O.CCNC(N)=O.CCO.CCOC(=O)CC(C)=O.O.O=Cc1ccccc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CCOC(=O)C1=C(C)N(CC)C(=O)NC1c1ccccc1Participants
7
Reactant 0
No Reactant data yet.
Product 1
Reagents, catalysts & solvents 6
Conditions
- Temperature
- 120 °C
Workup
- waitNo procedure recorded
- additionNo procedure recorded
- waitNo procedure recorded
- filtrationKeep solid
- washNo procedure recorded
- dry in vacuumNo procedure recorded
Sources & evidence
- ORD record
- ord-126472ce749542dc8113a70c68f056fd
- Source dataset
- Microwave-assisted Biginelli Condensation Dataset
- Original link
- View source
Reaction notes
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