Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)

HRID 10482

反応式

HRID 10482 の反応式
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9](#[N:12])[CH:10]=[CH2:11].CC(N=NC(C#N)(C)C)(C#N)C.P([O-])([O-])([O-])=O.[Ca+2].[Ca+2].[Ca+2].P([O-])([O-])([O-])=O>O>[CH2:11]=[CH:10][C:9]#[N:12].[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

参加物

6

反応物 4

HCID 6547AzobisisobutyronitrileHCID 7501StyreneHCID 7855AcrylonitrileHCID 24456Tricalcium Phosphate

生成物 1

HCID 62696Prop-2-enenitrile--ethenylbenzene (1/1)

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

71 parts of styrene, 29 parts of acrylonitrile, 120 parts of deionized water and 0.2 parts of azobisisobutylonitrile (AIBN) were blended. To the blend, 0.5 parts of tricalciumphosphate and 0.3 parts of mercaptan-containing chain transfer agent were added. The resultant solution was heated to 80° C. for 90 minutes and kept for 180 minutes. The resultant was washed, dehydrated and dried. Styrene-acrylonitrile copolymer (SAN) was obtained.

後処理

  1. additionwere added
  2. washThe resultant was washed
  3. customdried

出典と根拠

ORDレコード
ord-32423f84d6c1444db24b353eaff2d0d9
出典データセット
uspto-grants-2006_08
特許番号
US07094818B2

関連ノート

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