反応式
[Na].ClC1C(S)=C(Cl)C(Cl)=C(Cl)C=1Cl.[N+]([O-])(O)=O.[S:18](=[O:22])(=[O:21])([OH:20])[OH:19].[S:23](=[O:26])(=[O:25])=[O:24]>>[OH:21][S:18]([OH:22])(=[O:20])=[O:19].[O:24]=[S:23](=[O:26])=[O:25]参加物
6
実験手順
reacting this sodium salt of pentachlorothiophenol with a mixed nitration acid comprising nitric acid and sulfuric acid (and, preferably, sulfur trioxide to form oleum) at a temperature from about 35° C. to about 110° C. to form pentachloronitrobenzene, the nitric acid being in molar excess of the pentachlorothiophenol.
出典と根拠
- ORDレコード
- ord-ef5d4417de7a4c94a97e21416b1302a2
- 出典データセット
- uspto-grants-1984_07
- 特許番号
- US04461918
関連ノート
読み込み中…