N-Methylbenzamide → N-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
反応式
CNC(=O)c1ccccc1>C1=CCCC=CCC1.C1=CCCC=CCC1.C1CCOC1.CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C.C[OH2+].C[OH2+].[Ir].[Ir].c1ccc(-c2ccccn2)nc1>CNC(=O)c1ccccc1B1OC(C)(C)C(C)(C)O1参加物
6
反応条件
- 温度
- 60 °C
実験手順
Isolated by chromatography using deactivated silica gel and ethyl acetate and petroleum ether (10:1 to 2:1) as the eluent.
出典と根拠
- ORDレコード
- ord-ecb1fa564c574c269daf0952df1a6889
- 出典データセット
- Borylation dataset from Roche
反応ノート
読み込み中…