Boric Acid → 4,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL

HRID 1491511

反応式

HRID 1491511 の反応式
[B:1]([OH:4])([OH:3])[OH:2].[CH3:5][C:6](O)([CH2:8][CH:9](O)[CH3:10])[CH3:7]>CCCCCCC>[OH:2][B:1]1[O:4][C:6]([CH3:7])([CH3:5])[CH2:8][CH:9]([CH3:10])[O:3]1

参加物

4

反応物 2

HCID 7628Boric AcidHCID 7870Hexylene Glycol

生成物 1

HCID 3525154,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL

試薬・触媒・溶媒 1

HCID 8900Heptane溶媒

反応条件

温度
95 °C

実験手順

61.2 g of boric acid (1 mol) and 118.2 g of 2-methyl-2,4-pentanediol (1 mol) and 200 ml of heptane are charged to a reaction flask equipped with stirrer, Marcusson apparatus and reflux condenser. The reaction mixture is heated up to its reflux temperature (about 95° C.), with stirring, and is kept at that temperature for a 4-hour period.

後処理

  1. customequipped with stirrer
  2. temperatureMarcusson apparatus and reflux condenser
  3. temperatureThe reaction mixture is heated up to its
  4. waitis kept at that temperature for a 4-hour period

出典と根拠

ORDレコード
ord-eaeb699ad1e74e04bbf19442810f1b08
出典データセット
uspto-grants-1994_12
特許番号
US05370807

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