N,N,N-trimethylglycinium → 2-Amino-5-(hydroxymethyl)phenol

HRID 1764939

反応式

HRID 1764939 の反応式
[C:1](O)(=O)[CH2:2][C:3]([CH2:8][C:9]([OH:11])=O)([C:5]([OH:7])=O)O.CCOCCOCCO.C(O)(=O)CCCCCCC/C=C\CCCCCCCC.C(O)C(O)C.[CH3:48][N+:49](CC(O)=O)(C)C.CCCCCCCC/C=C\CCCCCCCCOCCOCCO.C([O-])(=O)C=C.S([O-])([O-])=O.[Na+].[Na+].C(N(CC(O)=O)CC(O)=O)CN(CC(O)=O)CC(O)=O.O=C1O[C@H]([C@H](CO)O)C(O)=C1O.[OH-].[NH4+]>O>[NH2:49][C:48]1[CH:1]=[CH:2][C:3]([CH2:5][OH:7])=[CH:8][C:9]=1[OH:11]

参加物

13

反応物 11

HCID 248N,N,N-trimethylglyciniumHCID 311Citric Acid2 回HCID 1030Propylene GlycolHCID 6049Ethylenediaminetetraacetic AcidHCID 8146Diethylene Glycol Monoethyl EtherHCID 14923Ammonium HydroxideHCID 24437Sodium SulfiteHCID 25188AcrylateHCID 445639Oleic Acid2 回HCID 133874552-((Z)-Octadec-9-enoxy)ethanolHCID 54670067L-Ascorbic Acid

生成物 1

HCID 145201152-Amino-5-(hydroxymethyl)phenol

試薬・触媒・溶媒 1

HCID 962Water溶媒3 回

反応条件

温度
40 °C

実験手順

To prepare pre-mix: Add to a suitable vessel in the following order, citric acid, ethoxy diglycol, oleic acid, propylene glycol, and cocaamidopropyl betaine, then agitate until fully dispersed, then add Oleth-10, Oleth-2 and acrylate co-polymers, continue the agitation for 10 minutes and transfer to main vessel. To the main vessel then add water (heated to 50° C.), oleic acid, water, sodium sulphite, and EDTA. Next weigh out and add the ascorbic acid, then stir well until dissolved. Separately weigh dyes into a clean beaker and transfer also to the main vessel. Add the dyes and stir until dissolved (heat to 40° C. as necessary). Cool to room temperature with stirring, add the ammonium hydroxide and water with stirring, add citric acid to pH 10, and transfer to the storage container.

後処理

  1. customTo prepare
  2. additionpre-mix
  3. additionuntil fully dispersed
  4. additionadd Oleth-10
  5. customfor 10 minutes
  6. stirringstir well
  7. dissolutionuntil dissolved
  8. additionAdd the dyes
  9. stirringstir
  10. dissolutionuntil dissolved
  11. temperatureCool to room temperature
  12. stirringwith stirring
  13. stirringwith stirring

出典と根拠

ORDレコード
ord-ec86bb39d47742e1b10cea3944d69566
出典データセット
uspto-grants-2007_06
特許番号
US07226487B2

関連ノート

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