Hydroquinone → tert-Butyl peroxybenzoate

HRID 1858054

反応式

HRID 1858054 の反応式
C[O-].[Na+].[O-2].[Al+3].[O-2].[O-2].[Al+3].C1(C=CC(O)=CC=1)[OH:10].CCC(OOC(OO)(CC)C)(OO)C.CN(C)C1C=CC=CC=1.[C:40]([O:49][O:50][C:51]([C:54]1[CH:59]=[CH:58][CH:57]=[CH:56][CH:55]=1)(C)C)([C:43]1C=CC=CC=1)([CH3:42])[CH3:41].C(OCCOCCOC(=O)C=C)(=O)C=C>ClCCl.C1(C)C=CC=CC=1>[C:40]([O:49][O:50][C:51](=[O:10])[C:54]1[CH:59]=[CH:58][CH:57]=[CH:56][CH:55]=1)([CH3:43])([CH3:42])[CH3:41]

参加物

10

反応物 7

HCID 785HydroquinoneHCID 949N,N-DimethylanilineHCID 6641Dicumyl peroxideHCID 19996Diethylene glycol diacrylateHCID 3672772Methyl ethyl ketone peroxideHCID 9989226AluminaHCID 10942334Sodium Methoxide

生成物 1

HCID 11966tert-Butyl peroxybenzoate

試薬・触媒・溶媒 2

HCID 1140Toluene溶媒HCID 6344Dichloromethane溶媒

実験手順

Sodium methoxide (NaOCH3), toluene (anhydrous), dichloromethane, hexanes, activated neutral aluminum oxide (60 to 50 mesh), hydroquinone, methyl ethyl ketone peroxide, dimethylaniline, dicumylperoxide, diethylene glycol diacrylate, and tert-butylperoxybenzoate were obtained from commercial sources and used as received.

出典と根拠

ORDレコード
ord-1b265212be2f48a2b206a49a2742bb59
出典データセット
uspto-grants-2000_11
特許番号
US06150429

関連ノート

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